e-journal

Catalytic properties of nano-sized ZSM-5 aggregates

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Abstract.
Nano-ZSM-5 (NZ) with well-defined porosity was synthesized by organic silica method. The material
exhibited more than a twofold increase in pore volume when compared to the normal ZSM-5 (HZ). The
increase in pore volume is observed in the entire range of the pores with diameter from 5A˚ to 1500A˚ . The
order of increase in volume is macropores (>500A˚ ) > micropores (up to 20A˚ ) > mesopores (20–500A˚ ).
Although macropore and mesopore formation is responsible for the major increase in the pore volume,
significant increase in zeolitic pore volume was also observed in NZ. Both the ZSM-5 materials were
tested for esterification of cyclohexanol with acetic acid under autogeneous pressure conditions where
NZ showed better activity (69% conversion).

Keywords:
ZSM-5
Mesoporosity
Micropore volume
t-Plot and adsorption isotherms

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Informasi Detail

Judul Seri

Catalysis Today

No. Panggil

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Penerbit

London : Elsevier B.V.., 2009

Deskripsi Fisik

Catalysis Today 141 (2009) 182–186

Bahasa

English

ISBN/ISSN

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Klasifikasi

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Tipe Isi

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Tipe Media

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Tipe Pembawa

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Edisi

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Subjek

KIMIA

Info Detail Spesifik

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Pernyataan Tanggungjawab

agus

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