KOH-catalyzed synthesis of biodiesel was carried out in capillary microreactors with inner diameters of 0.25 or 0.53 mm, with unrefined rapeseed oil and cottonseed oil as raw materials. The influences of the methanol to oil molar ratio, the residence time, the catalyst concentration, the reaction temperature, and the dimension of the capillary on the production of biodiesel were examined. The…
The transesterification of triacetin to methyl acetate catalyzed by 11 kinds of low boiling point amines was examined at subcritical methanol temperature as model reactions to simulate the biodiesel production. It was found that the branched amines showed higher yield of methyl acetate than normal amines. For normal amines, the yield of methyl acetate decreased with the increase of the carbo…