Abstract. Mesoporous titanosilicates with high titanium content were synthesized under mild acidic conditions (pH = 4.4, HAc–NaAc buffer solution) by co-condensation of acetylacetone-modified titanium isopropoxide (Ti(OBun)3 (acac)) and mixture of sodium silicate with tetramethoxysilane (TMOS) or tetraethoxysilane (TEOS) or tetrakis(2-hydroxyethyl)orthosilicate (EGMS), using block copolym…