A new cyanate ester functionalized polyhedral oligomeric silsesquioxane (POSS-Cy) monomer was prepared by reacting hydroxyl functionalized POSS-OH with cyanogen bromide (CNBr) in the presence of triethylamine (Et3N). The precursor POSS-OH and the corresponding cyanate ester POSS-Cy were characterized by Fourier transform infrared (FTIR), 1H and 13C nuclear magnetic resonance (13C-NMR) spectral …