Abstract. H1−xLaNb2−xMoxO7 was prepared by solid-state reaction followed by an ion-exchange reaction. Pt was incorporated in the interlayer of H1−xLaNb2−xMoxO7 by the stepwise intercalation reaction. The H1−xLaNb2−xMoxO7 showed hydrogen production activity and the activities were greatly enhanced by Pt co-incorporating. The x value in H1−xLaNb2−xMoxO7 had an important effect…